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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
temperature of decomposition (state purity)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
September 08, 2021 - September 23, 2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
EC No. 440/2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Key result
Decomposition:
yes
Decomp. temp.:
>= 190 °C
Remarks on result:
not determinable

Individual results:


Boiling point / boiling range: DSC measurement:


A measurement (see endpoint melting point) in aluminium crucibles with a hole showed no endothermal effect after the melting at 133 to 170°C up to a final temperature (500 °C). After melting the test item decomposed starting at approx. 200 °C.


Results of the capillary method


































No.






Set point /
°C



Heating rate / K/min



End
point /
°C



Remarks



1



120



1



200



136.7 °C: test item appeared wet


Approx. 160 °C: half of the test item appeared melted


169.7 °C: red melt


Approx. 190 °C: test item darkened to dark red



2



120



1



200



135.5 °C: test item started to melt


159.5 °C: half of the test item appeared melted


165.3 °C: red melt


Approx. 190 °C: test item darkened to dark red



3



120



1



200



133.3 °C: test item started to melt


155.3 °C: half of the test item appeared melted


163.9 °C: red melt


Approx. 190 °C: test item darkened to dark red



 


The test item had no boiling point under atmospheric conditions. Decomposition started at approx. 200 °C[1].


[1] Not valid as a study result on thermal stability

Conclusions:
The substance decomposes prior to boiling
Executive summary:

The boiling point of the test item was measured by DSC-measurements.


The test item Disperse Red 153 had a no boiling point according to European Commission Regulation (EC) No. 440/2008, A.2. as well as OECD 103 (1995).

Description of key information

The boiling point of the test item was measured by DSC-measurements.


The test item Disperse Red 153 has no boiling point according to European Commission Regulation (EC) No. 440/2008, A.2. as well as OECD 103 (1995).

Key value for chemical safety assessment

Temperature of decomposition (state purity):
190 °C

Additional information

The test item Disperse Red 153 has no boiling point, it discomposes prior to boiling.