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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
no
Type of method:
thermal analysis
Melting / freezing pt.:
-14.5 °C
Atm. press.:
1 013 hPa
Decomposition:
no

Two individual measurements were made, both yielding freezing points of -14.5 °C.

Conclusions:
The freezing point of the substance is -14.5 °C at standard atmospheric pressure.
Executive summary:

The freezing point of the test substance was determined in accordance with EU Method A.1. Test substance was filled into a solidification tube with a diameter ranging from 18 to 25 mm. The substance was then cooled down and stirred slowly and continuously with a precision thermometer (Amarell, serial number 8442, range -30 to +30 °C, fractional division 0.1 °C, uncertainty 0.03 °C). The freezing point is reached when the temperature remains constant. The freezing point was determined to be -14.5 °C under atmospheric pressure of 1013 hPa.

Description of key information

-14.5 °C

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-14.5 °C

Additional information

The freezing point of the test substance was determined in accordance with EU Method A.1 to be -14.5 °C. This value is supported by handbook data reporting a freezing point in the range of -12.4 to -15 °C.