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Diss Factsheets

Administrative data

Endpoint:
density
Remarks:
density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
19 June 2006 and 21 June 2006
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2006

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pycnometer method
Remarks:
Gas comparison pycnometer

Test material

Constituent 1
Reference substance name:
LiTOFA
IUPAC Name:
LiTOFA
Details on test material:
Sponsor's identification :Reaction salt of lithium hydroxide and tall oil fatty acids (LiTOFA)
Description : off-white solid
Lot number : LiTOFA_a01
Date received: 20 October 2005
Storage conditions :room temperature in the dark.

Results and discussion

Density
Type:
density
Density:
1 040 kg/m³
Temp.:
20 °C

Any other information on results incl. tables

Calibration

The pressure readings (P1and P2) and the calculated volume for the calibration ball are shown in the following table:

Determination

P1

P2

Volume (cm3)

Certified Volume (cm3)

Tolerance

(cm3)

A

17.091

8.461

56.5

56.6

± 0.5

B

17.234

8.531

56.4

56.6

± 0.5

Sample

The pressure readings, calculated volumes and density values obtained for the test material are shown in the following table:

Determination

P1

P2

Volume (cm3)

Density

(kg/m3)

A

17.075

6.889

14.7

1.04 x 103

B

17.157

6.921

14.7

1.04 x 103

Temperature:               20.0 ± 0.5ºC
Mean density:              1.04 x 103 kg/m3

Applicant's summary and conclusion

Conclusions:
The density of the test material has been determined to be 1.04 x 103 kg/m3 at 20.0 ± 0.5°C.
Executive summary:

Method

The density of liquids and solids was determined using a gas comparison pycnometer, Method 109 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Procedure

Testing was carried out using a Quantachrome MVP-2 gas comparison pycnometer.

Conclusion

The density of the test material has been determined to be 1.04 x 103 kg/m3 at 20.0 ± 0.5°C.