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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
16th Aug. 2017 - 21th Feb. 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions - Method A: Particle Size Distribution (effective hydrodynamic radius)
Deviations:
not specified
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7520 (Particle Size, Fiber Length, and Diameter Distribution)
Deviations:
not specified
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Deviations:
not specified
GLP compliance:
yes (incl. QA statement)
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution
Mass median aerodynamic diameter:
244.4 µm
Key result
Percentile:
D50
Mean:
244.4 µm
Remarks on result:
other: average of two test series of 3 measurmenets each; St. deviation not given
Percentile:
D10
Mean:
31 µm
Remarks on result:
other: average of two test series of 3 measurmenets each; St. deviation not given
Percentile:
D90
Mean:
854.8 µm
Remarks on result:
other: average of two test series of 3 measurmenets each; St. deviation not given

Particle Size Distribution

Two test series of 3 measurements each were performed with the test item.

Figure 1 and Figure 2 show the results of both test series. On the left y-axis the fraction distribution and on the right y-axis the cumulative distribution is shown.

 

Test series 1 (Figure 1):

D10:       31.1 µm

D50:       241.8 µm        (Median diameter)

D90:       827.8 µm

 

Test series 2 (Figure 2):

D10:       30.9 µm

D50:       247.0 µm        (Median diameter)

D90:       881.7 µm

 

Average

D10:       31.0 µm

D50:       244.4 µm        (Median diameter)

D90:       854.8 µm

Conclusions:
Median particle size D50 = 244.4 µm (laser diffraction measurements)
Executive summary:

The test item has a median particle size D50 = 244 µm, which was determined by laser diffraction measurement.

Description of key information

Median particle size D50 = 244.4 µm (laser diffraction measurements)

Additional information