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Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing conducted between 16 May 2008 and 02 Sepetember 2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted to GLP and in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not effect the quality of the relevant results.
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
ASTM E537-76
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Boiling pt.:
>= 602 - <= 644 K
Atm. press.:
101.6 kPa
Decomposition:
no

Results from dertemination 1 and 2 are shown below as follows:

Thermographic - Data - determination 1 at 101.6Kpa atmospheric pressure.

Thermal Event

Interpretation

Temperature

°C

K

Endotherm

Onset of boiling temperature

329.23

602.38

Peak boiling temperature

350.34

623.58

Endset of boiling temperature

370.68

643.83

 

Thermographic - Data - determination 2 at 101.6Kpa atmospheric pressure.

Thermal Event

Interpretation

Temperature

°C

K

Endotherm

Onset of boiling temperature

328.61

601.76

Peak boiling temperature

349.58

622.73

Endset of boiling temperature

370.13

643.28

Overall boiling range: 602 to 644 +/- 0.5K

Conclusions:
The boiling range of the test material has been determined to be 602 to 644 +/- 0.5K at 101.6 kPa
Executive summary:

Method:

The determination was carried out by differential scanning calorimetry (DSC) using the procedure specified in ASTM E537 -76, Method A2 of Commisision Directive 92/69/EEC (which constitutes Annex V of Council Directive 67/548/EEC).

Result:

The boiling range of the test material has been determined to be 602 to 644 K at 101.6 kPa

Description of key information

The determination was carried out by differential scanning calorimetry (DSC) using the procedure specified in ASTM E537 -76, Method A2 of Commission Directive 92/69/EEC.

The boiling range of the test material has been determined to be 602 to 644 K at 101.6 kPa

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
602 K

Additional information