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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
24 Nov. - 29. Nov. 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions) - Method B: Fibre Length and Diameter Distributions
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Version / remarks:
2009
GLP compliance:
yes (incl. QA statement)
Remarks:
Hess. Ministerium für Umwelt, Energie, Landwirtschaft und Verbraucherschutz, Wiesbaden, Germany
Type of method:
Laser scattering/diffraction
Type of particle tested:
other: slightly transparent particles of irregular shape
Type of distribution:
volumetric distribution
Mass median aerodynamic diameter:
ca. 20.3 µm
Percentile:
D10
Mean:
1.7 µm
St. dev.:
0
Key result
Percentile:
D50
Mean:
12.1 µm
St. dev.:
0
Percentile:
D90
Mean:
163.3 µm
St. dev.:
0

Two test series of three measurements each were performed.

Test series

D10(µm)

D50(µm)

D90(µm)

1

1.7

12.2

165.2

2

1.7

11.9

161.3

Mean

1.7

12.1

163.3

 

The mass median aerodynamic diameter was calculated by using the results of the particle size distribution and the determination of the relative density by following equation:

 

              MMAD = D50* (ρ/K)0.5

with

              D50 = volume median diameter (VMD)

              ρ = particle density

              K = shape factor (1 for spheric particles)

Description of key information

L50 = 12.1 µm (OECD 110, GLP)

Additional information

particle size distribution by laser diffraction