Registration Dossier
Registration Dossier
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EC number: 812-378-1 | CAS number: 210420-85-2
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- From 18 November 2016 to 23 March 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 017
- Report date:
- 2017
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Version / remarks:
- 2008
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Version / remarks:
- 1995
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EPA OPPTS 830.7200 (Melting Point / Melting Range)
- Version / remarks:
- 1998
- Deviations:
- no
- GLP compliance:
- yes
- Type of method:
- differential scanning calorimetry
Test material
- Reference substance name:
- Reference substance 001
- Cas Number:
- 210420-85-2
- Reference substance name:
- N-methyldidecylamine
- EC Number:
- 230-990-1
- EC Name:
- N-methyldidecylamine
- Cas Number:
- 7396-58-9
- Molecular formula:
- C21H45N
- IUPAC Name:
- N-decyl-N-methyldecan-1-amine
- Reference substance name:
- Water
- EC Number:
- 231-791-2
- EC Name:
- Water
- Cas Number:
- 7732-18-5
- Molecular formula:
- H2O
- IUPAC Name:
- Dihydrogen oxide
- Reference substance name:
- Unknown impurities
- Molecular formula:
- Not available
- IUPAC Name:
- Unknown impurities
- Test material form:
- solid
- Details on test material:
- - Appearance: Slightly yellow gel
- Storage conditions: At room temperature; container flushed with nitrogen
Constituent 1
Constituent 2
Constituent 3
impurity 1
Results and discussion
Melting / freezing point
- Key result
- Decomposition:
- yes
- Decomp. temp.:
- > 100 °C
- Remarks on result:
- other: no melting point
Any other information on results incl. tables
TGA EXPERIMENT (PRELIMINARY TEST)
From 100°C upwards the weight of the sample decreased significantly. At 256°C the sample weight had decreased by 25%. After the experiment, a colourless molten residue remained in the sample container (original colour: slightly yellow). The change of the colour indicated reaction and/or decomposition.
DSC EXPERIMENTS
In none of the experiments, effects were observed due to melting (or boiling) during cooling and heating. The residue at the end of each test was molten and colourless. The colour change may be due to reaction/decomposition and/or evaporation of part of the substance. DSC curve of Experiment 1 is shown below.
Applicant's summary and conclusion
- Conclusions:
- The substance has no melting temperature.
- Executive summary:
Differential Scanning Calorimetry (DSC) experiments were performed in a GLP study according to EC A.1, OECD 102 and OPPTS 830.7200.
Reaction/decomposition and/or evaporation of the substance starts at ca 100°C. Melting of the substance was not observed below the temperature at which reaction/decomposition and/or evaporation started. The substance has no melting temperature.
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
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