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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
05 Sep 2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2020
Report date:
2020

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
yes
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
Reaction mass of (((1,3-phenylenebis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(ethane-2,1-diyl) bis(2-methylacrylate) and (1,3-phenylenebis(oxy))bis(propane-3,1-diyl) bis(2-methylacrylate) and 3-(3-(2-(2-(methacryloyloxy)ethoxy)ethoxy)phenoxy)propyl methacrylaterate
EC Number:
944-271-1
Cas Number:
2305048-54-6
Molecular formula:
not applicable for multi-constituent.
IUPAC Name:
Reaction mass of (((1,3-phenylenebis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(ethane-2,1-diyl) bis(2-methylacrylate) and (1,3-phenylenebis(oxy))bis(propane-3,1-diyl) bis(2-methylacrylate) and 3-(3-(2-(2-(methacryloyloxy)ethoxy)ethoxy)phenoxy)propyl methacrylaterate
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Lot/batch number of test material: 653940
- Purity, including information on contaminants, isomers, etc.: 100% UVCB (45.11% DiBrOE2RMA; 32.31% DiBrORMA; 15.24% DiBrE4RMA)
- Expiration date: February 2020

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Stored at room temperature in a dark, ventilated cabinet in the original container

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
-42.56 °C

Any other information on results incl. tables

 Sample Type  Weight of Sample (mg)  Onset Temp (°C)
 5 °C/min  1.112  -43.23
10 °C/min  5.686  -42.23
 10 °C/min 3.120   -42.08
 10 °C/min  2.578  -41.64
 5 °C/min  2.832  -43.18
 5 °C/min  4.400  -42.98
    Mean:  -42.56
 SD:  0.663
 % RSD:  -1.56%

Applicant's summary and conclusion

Conclusions:
The melting point of DiBrORMA was determined to be -42.56 °C (OECD 102).
Executive summary:

The melting point of DiBrORMA was determined using differential scanning calorimetry (DSC). During the heating phase a distinct endothermic effect was observed. The standard deviation from onset temperature in the six tests was 0.663 °C from their mean value of -42.56 °C. The study was conducted in accordance with OECD 102 guidelines and was GLP compliant. Therefore, the study is considered reliable without restrictions.