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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2010-01-11 to 2010-01-20
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Remarks:
The study was conducted according to an internationally recognised method, and under GLP. However, the heating device and the heating rate were not conform to the recommendations. The test substance composition is adequately characterised with its purity. Therefore validation applies with restrictions.
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
27thJuly 1995
Deviations:
yes
Remarks:
heating device, heating rate
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
Council Regulation (EC) No 440/2008 dated30 May 2008
Deviations:
yes
Remarks:
heating device, heating rate
GLP compliance:
yes (incl. QA statement)
Remarks:
Inspected on 04th and 05th May 2009 / Signed on 1st September 2009
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
Storage condition of test material: Refrigerator (between 0 and 10°C under nitrogen)
Key result
Boiling pt.:
337 °C
Atm. press.:
97.2 kPa

Preliminary test: 610 K (337°C) at 97.2 kPa

Determination 1: 610 K (337°C) at 97.2 kPa

Determination 2: 610 K (337°C) at 97.2 kPa

Precision +/- 2 K

Executive summary:

The boiling point of the test substance was measured under GLP according to OECD 103 / EU A2 guideline, Siwoloboff (capillary) method.

Two determinations were performed; individual results were found to fall within accuracy, therefore the mean value is retained.

The boiling point of the test substance is 337°C under 97.2 kPa.

Description of key information

Boiling point = 337°C (under 97.2 kPa)

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
337 °C

Additional information

A reliable study, conducted according to a recognized OECD/EC method and under GLP, is available. Despite restrictions regarding the procedure, it is considered as a key study. The result is retained as key data.