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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
27.9.2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2019
Report date:
2019

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
474-080-4
EC Name:
-
Cas Number:
76801-93-9
Molecular formula:
C14H18I3N3O6
IUPAC Name:
5-amino-N1,N3-bis(2,3-dihydroxypropyl)-2,4,6-triiodobenzene-1,3-dicarboxamide
impurity 1
Reference substance name:
Unknown impurities
Molecular formula:
Not available
IUPAC Name:
Unknown impurities
Test material form:
solid
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: 00104016
- Expiration date of the lot/batch: 12/2020

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Store in cool place. Keep container tightly closed in a dry and well-ventilated place.
- Stability under test conditions: Stable

Results and discussion

Boiling point
Decomposition:
yes
Decomp. temp.:
> 235 °C

Applicant's summary and conclusion

Conclusions:
The thermal decomposition of test item was observed above 235 °C, i.e. 508 K. No peak corresponding to boiling of test item was observed to the temperature at which the thermal decomposition started. The boiling temperature of test item, ATIBA-A, could not be determined due to thermal decomposition of test item.
Executive summary:

The boiling temperature of test item, ATIBA-A, was investigated. The Differential Scanning Calorimetry method was used. The thermal decomposition of test item was observed above 235 °C, i.e. 508 K. No peak corresponding to boiling of test item was observed to the temperature at which the thermal decomposition started. The boiling temperature of test item, ATIBA-A, could not be determined due to thermal decomposition of test item.