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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016-10-28 to 2016-11-01
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
2008
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
< -100 °C
Atm. press.:
>= 1 017 - <= 1 021 hPa
Remarks on result:
other: the test item has no melting point down to -100 °C

The substance is liquid at room temperature.

During the cooling and the subsequent heating phase, no thermal effects were observed in the temperature range from -100 to 25 °C. It can be assumed that the test item has no melting or freezing point in this temperature range. Therefore the test item has no melting point down to a temperature of -100 °C.

In the temperature range of 10 – 330 °C an endothermic effect (boiling) was observed. No further thermal effects were observed up to the test end temperature of 500 °C.

Replicate

Sample weight / mg

Onset of Effect / °C

Range of effect / °C

Weight loss / mg

Atmospheric pressure / hPa

1

16.19

108.51

10–330(endo)

16.19

1020.7

2

13.39

110.88

40–330(endo)

13.34

1016.7

Conclusions:
The test item has no melting point down to -100 °C at atmospheric pressure (1017 hPa and 1021 hPa, respectively) as determined by differential scanning calorimetry.
Executive summary:

The melting point of the test item was assessed according to OECD 102, by differential scanning calorimetry.

During the cooling and the subsequent heating phase, no thermal effects were observed in the temperature range from -100 to 25 °C. It can be assumed that the test item has no melting or freezing point in this temperature range. Therefore the test item has no melting point down to a temperature of -100 °C.

In the temperature range of 10 - 330 °C an endothermic effect (boiling) was observed. No further thermal effects were observed up to the test end temperature of 500 °C.

Description of key information

For this endpoint one experimental study is available, which has been conducted according to OECD 102, differential scanning calorimetry. The test item has no melting point down to a temperature of -100 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-100 °C

Additional information

The test item has no melting point down to a temperature of -100 °C.