Registration Dossier
Registration Dossier
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 229-390-2 | CAS number: 6505-30-2
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Qualifier:
- according to guideline
- Guideline:
- EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
- GLP compliance:
- yes (incl. QA statement)
- Other quality assurance:
- other: SOP-LA-021
- Remarks:
- Boiling point by DSC
- Type of method:
- differential scanning calorimetry
- Atm. press.:
- 1 004.3 hPa
- Decomposition:
- yes
- Remarks:
- No boiling was detected of the test item up to its decomposition.
- Decomp. temp.:
- >= 200 °C
- Remarks on result:
- other: PN15834
- Remarks:
- The test item showed an endothermic effect. Onset of effect 469.63°C. Range of effect 460 - 480°C (endo).
- Atm. press.:
- 1 003.6 hPa
- Decomposition:
- yes
- Remarks:
- No boiling was detected of the test item up to its decomposition.
- Decomp. temp.:
- >= 200 °C
- Remarks on result:
- other: PN15839
- Remarks:
- The test item showed an endothermic effect. Onset of effect 465.94°C. Range of effect 290 - 490°C (endo).
- Conclusions:
- No boiling point of the test item was observed up to its decomposition starting from 200°C.
- Executive summary:
The boiling point of the test item Hydrogen [4-[[4-diethylamino)phenyl][4-[ethyl[(3-sulphonatobenzyl)amino]-o-tolyl]methylene]-3-methylcylohexa-2,5-dien-1-ylidene](ethyl)3-sulphonatobenzyl)ammonium, sodium salt was investigated by differential scanning calorimetry (DSC) method according to Regulation EC No. 440/2008 Method A.2., OECD Test Guideline 103 (1995) and EPA OCSPP 830.7220 (1996). No boiling point up to its decomposition starting at a temperature of approx. 200 °C was determined.
Reference
The thermograms of the DSC runs PN15834 and PN15839 are shown in Figure 2 and Figure 3, respectively. In the temperature range of 200 – 270 °C the test item showed an exothermic effect with a mean energy release of -140 J/g. The test item showed an endothermic effect in the temperature range of 460 – 490 °C.
Table 1: Results of the DSC-measurements
| No. | Sample weight / mg | Onset of Effect / °C | Range of Effect / °C | Weight loss / mg | Atmospheric pressure / hPa |
| PN15834 | 11.63 | --- 469.63 |
210 - 280 (exo) 460 - 480 (endo) |
5.94 | 1004.3 |
| PN15839 | 13.66 | --- 465.94 |
210 - 280 (exo) 290 - 490 (endo) |
8.35 | 1003.6 |
During the heating an exothermic effects was detected. No melting or boiling was detected of the test item.
Description of key information
The boiling point of the test item was investigated by differential scanning calorimetry method according to Regulation EC No. 440/2008 Method A.2., OECD Test Guideline 103 (1995) and EPA OCSPP 830.7220 (1996). No boiling point up to its decomposition starting at a temperature of approx. 200 °C was determined.
Key value for chemical safety assessment
- Boiling point at 101 325 Pa:
- 200 °C
Additional information
"Should read: > 200 °C"
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
