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Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
The study was conducted between 13 February 2018 and 30 March 2018.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
GLP compliance:
no
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
distillation method

Test material

Constituent 1
Chemical structure
Reference substance name:
2-[(2-hydroxyphenyl)methyl]phenol; 2-[(4-hydroxyphenyl)methyl]phenol; 4-[(4-hydroxyphenyl)methyl]phenol
EC Number:
908-912-9
Cas Number:
1333-16-0
Molecular formula:
C39H36O6
IUPAC Name:
2-[(2-hydroxyphenyl)methyl]phenol; 2-[(4-hydroxyphenyl)methyl]phenol; 4-[(4-hydroxyphenyl)methyl]phenol
Test material form:
solid
Specific details on test material used for the study:
Sample name: supplied as a name of Bisphenol-F(Reaction mass of 2,2'-methylenediphenol and 4,4'-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)
Appearance: Solid
Purity: 98%
CAS: 13316-0

Results and discussion

Boiling point
Key result
Boiling pt.:
291 °C
Atm. press.:
101.3 kPa

Any other information on results incl. tables

Boiling point

Boiling point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] (101.3 kPa)

Sample name

 

Temperature

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

 

°C

K

 

291

564

Note) Temperature in Kelvin (K) = Temperature in °C + 273.15

 

Boiling point result at atmospheric pressure (101.3 kPa)

Sample name

Run

Temperature

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

°C

K

1

293

566

2

289

562

Average

291

564

Note) Temperature in Kelvin (K) = Temperature in °C + 273.15

 

Distillation method can measure up to the maximum of 250 °C. The sample was not distilled even at 250 °C (523 K) by distillation apparatus.

As a result of DSC analysis, a volatile peak was observed at 293 °C and 289 °C for the first and second test respectively. The boiling point is reported as the average value of the test result of 291 °C.

After the test, the sample container was seemed empty.

Boiling point average: 291 °C (564 K)

Applicant's summary and conclusion

Conclusions:
Boiling point was measured by using a general distillation apparatus and DSC under atmospheric pressure. The by distillation apparatus could not measure the boiling point of the sample due to its limitations, and for the result of DSC analysis, the boiling point of the sample was 291 °C (564 K). Conclusively, boiling point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was 291 °C (564 K) at 101.3 kPa.
Executive summary:

The boiling point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was measured by distillation method and DSC using the procedure specified in Method 103 of the OECD test Guidelines for Testing of Chemicals, 27 July 1995.

The results of the study were as follows:

Boiling point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] (101.3 kPa)

Sample name

 

Temperature

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

 

°C

K

 

291

564

Note) Temperature in Kelvin (K) = Temperature in °C + 273.15

 

Boiling point result at atmospheric pressure (101.3 kPa)

Sample name

Run

Temperature

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

°C

K

1

293

566

2

289

562

Average

291

564

Note) Temperature in Kelvin (K) = Temperature in °C + 273.15

 

Distillation method can measure up to the maximum of 250 °C. The sample was not distilled even at 250 °C (523 K) by distillation apparatus.

As a result of DSC analysis, a volatile peak was observed at 293 °C and 289 °C for the first and second test respectively. The boiling point is reported as the average value of the test result of 291 °C.

After the test, the sample container was seemed empty.

Boiling point average: 291 °C (564 K)

Conclusion:

Boiling point was measured by using a general distillation apparatus and DSC under atmospheric pressure. The by distillation apparatus could not measure the boiling point of the sample due to its limitations, and for the result of DSC analysis, the boiling point of the sample was 291 °C (564 K). Conclusively, boiling point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was 291 °C (564 K) at 101.3 kPa.