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EC number: 908-912-9 | CAS number: 1333-16-0
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- The study was conducted 13 February 2018 and 30 March 2018
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 018
- Report date:
- 2018
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- GLP compliance:
- no
- Other quality assurance:
- ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
- Type of method:
- differential scanning calorimetry
Test material
- Reference substance name:
- 2-[(2-hydroxyphenyl)methyl]phenol; 2-[(4-hydroxyphenyl)methyl]phenol; 4-[(4-hydroxyphenyl)methyl]phenol
- EC Number:
- 908-912-9
- Cas Number:
- 1333-16-0
- Molecular formula:
- C39H36O6
- IUPAC Name:
- 2-[(2-hydroxyphenyl)methyl]phenol; 2-[(4-hydroxyphenyl)methyl]phenol; 4-[(4-hydroxyphenyl)methyl]phenol
- Test material form:
- solid
Constituent 1
- Specific details on test material used for the study:
- Sample name: supplied as a name of Bisphenol-F(Reaction mass of 2,2'-methylenediphenol and 4,4'-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)
Appearance: Solid
Purity: 98%
CAS: 1333-16-0
Results and discussion
Melting / freezing point
- Key result
- Melting / freezing pt.:
- 98.6 °C
- Atm. press.:
- 101.3 kPa
Any other information on results incl. tables
Melting point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]
Sample name |
Item |
Temperature |
|
°C |
K |
||
Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] |
Tm |
98.6 |
371.8 |
Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15
The sample was measured by differential scanning calorimeter (DSC)
Tm: melting temperature at 1stheating (peak maximum)
Results of DSC
Sample name |
Item |
Run |
Temperature |
|
Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] |
Tm |
°C |
K |
|
1 |
98.51 |
371.66 |
||
2 |
98.70 |
371.85 |
||
Average |
98.61 |
371.76 |
||
Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15
The sample was measured by differential scanning calorimeter (DSC)
Tm: melting temperature at 1st heating (peak maximum)
Applicant's summary and conclusion
- Conclusions:
- Melting temperature of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was (98.6 ± 0.5) °C {(371.8 ± 0.5) K} at 101.3 kPa by DSC.
- Executive summary:
The melting point of Bisphenol-F (Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was measured by differential scanning calorimeter (DSC) using the procedure specified in Method 102 of the OECD Test Guidelines for Testing of Chemicals, 27 July 1995.
The results of the study were as follows:
Melting point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]
Sample name
Item
Temperature
°C
K
Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]
Tm
98.6
371.8
Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15
The sample was measured by differential scanning calorimeter (DSC)
Tm: melting temperature at 1stheating (peak maximum)
Results of DSC
Sample name
Item
Run
Temperature
Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)
Tm
°C
K
1
98.51
371.66
2
98.70
371.85
Average
98.61
371.76
Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15
The sample was measured by differential scanning calorimeter (DSC)
Tm: melting temperature at 1st heating (peak maximum)
Conclusion:
Melting temperature of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was (98.6 ± 0.5) °C {(371.8 ± 0.5) K} at 101.3 kPa by DSC.
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