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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
This study was conducted between 01 June 2017 and 21 October 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: The study is considered to be a reliability 1 as it has been conducted according to OECD TG 102 using the method to determine the freezing point and in compliance with GLP.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
EC No. 440/2008 of 30 May 2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point
Specific details on test material used for the study:
Information as provided by the Sponsor.
Identification: 1,3-Benzenedimethanamine, reaction products with glycidyl tolyl ether
Appearance/Physical state: clear, colorless, viscous liquid
Batch: WA 1508
Purity: 100% UVCB
Expiry date: 01 January 2021
Storage conditions: room temperature, in the dark
Key result
Melting / freezing pt.:
0 °C

Preliminary Test

The stationary point of the preliminary test was -5.0 °C (268 K) and the pour point of the preliminary test was -2 °C (271 K).

Main Test

The results of the main test are shown in the following table:

Table 1

 

Determination 1

Determination 2

Stationary point (°C)

-3.0

-3.0

Pour point (°C)

0.0

0.0

Overall pour point result        :          0± 3 °C (276± 3 K)

 

Conclusions:
The pour point of the test item has been determined to be 0 ± 3 °C (273 ± 3 K).
Executive summary:

The general physico-chemical properties of 1,3-Benzenedimethanamine, reaction products with glycidyl tolyl ether have been determined. 

 

Melting/FreezingPoint.The test item was determined to have a pour point of 0 ± 3 °C (273 ± 3 K),determined using a procedure designed to be compatible with Method A.1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Description of key information

The test item was determined to have a pour point of 0 ± 3 °C (273 ± 3 K), determined using a procedure designed to be compatible with Method A.1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
0 °C

Additional information