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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Remarks:
only one measurement was performed; no reference material was subjected to the same controlled temperature programme
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
yes
Remarks:
only one measurement was performed; no reference material was subjected to the same controlled temperature programme
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
yes
Remarks:
only one measurement was performed; no reference material was subjected to the same controlled temperature programme
Principles of method if other than guideline:
The test was carried aout in a thermal analysis equipment of mettler Toledo, using TGA/STDA851e model.
GLP compliance:
no
Type of method:
thermal analysis
Key result
Melting / freezing pt.:
> 1 000 °C
Sublimation:
no
Remarks on result:
other: no significant thermal effects from 25 °C to 1000°C

The result is in accordance with the melting points of the detected phases rutile (m.p. 1843°C*), corundum (m.p. 2054°C*) and pseudobrookite (m.p. > 1600°C**).

* Lide, D.R. (Ed.) CRC handbook of chemistry and physics. 88th. pp 4 -96. Boca Raton: CRC, 2008

** Phase diagram 2170. In H.F. Mc Murdie, et al (Ed.). Phase diagrams from ceramists. Vol.II. The American Ceramic Society. Ohio. 1985.

Conclusions:
The test item has no melting point up to 1000 °C. No significant thermal effects from 25 °C to 1000 °C were determined in a differential thermal analysis.

Description of key information

The test item has no melting point up to 1000 °C. No significant thermal effects from 25 °C to 1000 °C were determined in a differential thermal analysis.

Key value for chemical safety assessment

Additional information