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EC number: 807-159-2 | CAS number: 69701-99-1
Auto flammability
Administrative data
Link to relevant study record(s)
- Endpoint:
- auto-ignition temperature (liquids)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 30 Nov 2017 - 06 Dec 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Specific details on test material used for the study:
- - Appearance/physical state: clear colorless liquid
- Batch: 09892701
- Purity: 99.9%
- Expiry date: 06 March 2018
- Storage conditions: room temperature, in the dark - Auto-ignition temperature:
- >= 255 - <= 265 °C
- Atm. press.:
- >= 102.4 - <= 103.2 kPa
- Conclusions:
- The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.
- Executive summary:
Introduction
The determination was carried out using a procedure* designed to be compatible with Method A.15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
Results
258°C No ignition. Grey fumes were emitted.
Auto-ignition temperature of 260 ± 5 °C.
Conclusion
The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.
Reference
Results of the auto-ignition temperature determination are shown in the following table:
| Temperature (ºC) | Clean Flask (Yes/No) |
Volume (µL) |
Ignition Delay (s) |
Observations |
| 200 | yes | 70 | >300 | No ignition. Grey fumes were emitted. |
| 250 | yes | 70 | >300 | No ignition. Grey fumes were emitted. |
| 300 | yes | 70 | 5 | An orange flame was observed. Grey fumes were emitted. |
| 280 | yes | 70 | 13 | An orange flame was observed. Grey fumes were emitted. |
| 270 | no | 70 | 16 | An orange/blue flame was observed. Grey fumes were emitted. |
| 260 | no | 70 | >300 | No ignition. Grey fumes were emitted. |
| 262 | no | 70 | >300 | No ignition. Grey fumes were emitted. |
| 266 | yes | 70 | >300 | No ignition. Grey fumes were emitted. |
| 268 | yes | 70 | >300 | No ignition. Grey fumes were emitted. |
| 268 | yes | 200 | 15 | An orange/blue flame was observed. Grey fumes were emitted. |
| 266 | yes | 200 | 16 | An orange/blue flame was observed. Grey fumes were emitted. |
| 262 | yes | 200 | 20 | An orange/blue flame was observed. Grey fumes were emitted. |
| 260 | yes | 200 | 20 | An orange/blue flame was observed. Grey fumes were emitted. |
| 250 | yes | 200 | >300 | No ignition. Grey fumes were emitted. |
| 252 | yes | 200 | >300 | No ignition. Grey fumes were emitted. |
| 256 | yes | 200 | >300 | No ignition. Grey fumes were emitted. |
| 258 | yes | 200 | >300 | No ignition. Grey fumes were emitted. |
| 258 | yes | 400 | >300 | No ignition. Grey fumes were emitted. |
| 258 | yes | 600 | >300 | No ignition. Grey fumes were emitted. |
| 258 | yes | 800 | >300 | No ignition. Grey fumes were emitted. |
| 258 | yes | 1000 | >300 | No ignition. Grey fumes were emitted. |
Room temperature: 19 °C
Atmospheric pressure: 102.4 to 103.2 kPa
Description of key information
The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.
Key value for chemical safety assessment
- Autoflammability / Self-ignition temperature at 101 325 Pa:
- 260 °C
Additional information
The determination of auto-ignition temperature of MEDOL-10 (Envigo Research Limited, 2018, Study MK65MG) was carried out using a procedure designed to be compatible with EC Method A.15. The test was conducted in compliance with GLP.
The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.
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