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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
from 2000-04-18 to 2000-07-14
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
92/69
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
GLP compliance:
yes
Type of method:
differential thermal analysis
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Batch No.of test material: 147-270300-1
Key result
Decomposition:
yes
Decomp. temp.:
85 °C
Remarks on result:
not determinable

The sample was closed up in a crucible made of aluminium with perforated lid and heated up in a DTA-system with a heating rate of 5 K/min. The boiling curve of the sample was a steep endothermic signal.

Conclusions:
Exothermal decomposition starts at 85 °C and there is no boiling point up to the decomposition of the test substance.
Executive summary:

A study was conducted according to Regulation (EC) No 92/69 method A.2 and OECD test guideline 103, to determine the boiling point of the test item using differential thermal analysis (DTA). The test item was weighed out in an aluminium crucible. The substance was heated at a constant heating rate of 5 K/min. At 85 °C decomposition began and till this temperature no boiling was observed. No observations were made which cause doubt on the validity of the outcome of the study.

Description of key information

The test item decomposes at 85 °C. Thus, no boiling point can be defined.

Key value for chemical safety assessment

Additional information

A study was conducted according to Regulation (EC) No 92/69 method A.2 and OECD test guideline 103, to determine the boiling point of the test item using differential thermal analysis (DTA). The test item was weighed out in an aluminium crucible. The substance was heated at a constant heating rate of 5 K/min. At 85 °C decomposition began and till this temperature no boiling was observed. No observations were made which cause doubt on the validity of the outcome of the study.