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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
12.03.-26.06.2014
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
> 428 - < 433 °C
Atm. press.:
1 013 hPa
Decomposition:
no

Two measurements in aluminum crucibles with a hole showed an endothermic effect (boiling) in the temperature range 365-445 °C with an onset temperature between 427.9-433.0 °C. The onset temperature is derived from the intersection of the tangent line with the highest slope of the endothermic peak with the baseline. The DSC run no. 34306 showed a small additional endothermic signal in the temperature range of 375 - 385 °C.

 

ID

Onset/ °C

Temperature range/ °C

Crucible

34306

433.02

385 - 445

Aluminum with a hole

34305

427.89

365 - 440

Aluminum with a hole

 

Conclusions:
The test item has a boiling range of 428 - 433 °C.
Executive summary:

A study was conducted according to Regulation (EC) No 440/2008 method A.2 to determine the boiling point of the test item using differential scanning calorimetry.

Two measurements in aluminium crucibles with a hole showed an endothermic effect (boiling) in the temperature range 365-445 °C with an onset temperature between 427.9-433.0 °C. The test item has a boiling range of 428 - 433 °C.

Description of key information

The boiling point of the test substances ranges from 428 -433°C.

Key value for chemical safety assessment

Additional information

A study was conducted according to Regulation (EC) No 440/2008 method A.2 to determine the boiling point of the test item using differential scanning calorimetry.

Two measurements in aluminium crucibles with a hole showed an endothermic effect (boiling) in the temperature range 365-445 °C with an onset temperature between 427.9-433.0 °C. The test item has a boiling range of 428 - 433 °C.