Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
14.02.2002
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002
Report date:
2002

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
451-510-9
EC Name:
-
Cas Number:
128446-33-3
Molecular formula:
C36H42O12(OH)18-y[(C3H6O)nOH]; y=1-10; n=1-4; y x n = 3,7 (average)
IUPAC Name:
Reaction products of .alpha.-cyclodextrin and methyloxirane
Details on test material:
Batch 63B001
Purity 95.9 %

Results and discussion

Melting / freezing point
Key result
Decomposition:
yes
Decomp. temp.:
>= 200 - <= 540 °C
Sublimation:
no

Any other information on results incl. tables

No melting peak (endothermic reaction) in DSC was observed.

Between 200 °C and 540 °C the DSC showed exothermic peaks with different intensity, which indicated further decomposition of the test substance. A loss of mass began at about 290 °C. At 540 °C about 98 % of the initial mass was lost.

Applicant's summary and conclusion

Conclusions:
A melting point cannot be determined.