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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
December 29th, 2015.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method
Key result
Melting / freezing pt.:
>= 135.2 - <= 136.7 °C
Atm. press.:
107.5 kPa
Decomposition:
no
Sublimation:
no

Table 1. The observed values of melting point.

Sample

Visually

Automatically

Atmospheric pressure, hPa

 Initial value of the melting point, °C

Final value of the melting point, °C

Final value of the melting point, °C

1

135.2

136.1

136.7

1007.5

2

135.2

136.1

136.7

3

135.3

136.1

136.7

Average values ± standard deviations, °C

135.2 ± 0.1

136.1 ± 0.0

137.6 ± 0.3

Conclusions:
The melting point of the test item was observed in the temperature range of 135.2 –136.7 °C.
Executive summary:

The study to determine the melting point of the test item was performed according to OECD 102, under GLP conditions. The melting point of the test substance was observed in the temperature range of 135.2 –136.7 °C.

Description of key information

Key study. Method according to OECD 102, GLP study. The melting point of the test substance was observed in the temperature range of 135.2 –136.7 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
135.2 °C

Additional information