Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2009
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2-bis({[3-(4-ethylpiperazin-1-yl)propanoyl]oxy}methyl)butyl 3-(4-ethylpiperazin-1-yl)propanoate
EC Number:
700-404-3
Cas Number:
127929-37-7
Molecular formula:
C33H62N6O6
IUPAC Name:
2,2-bis({[3-(4-ethylpiperazin-1-yl)propanoyl]oxy}methyl)butyl 3-(4-ethylpiperazin-1-yl)propanoate

Results and discussion

Boiling point
Boiling pt.:
>= 278.2 - <= 278.4 °C
Atm. press.:
>= 101 100 - <= 101 101 Pa

Any other information on results incl. tables

A change in colour from brown-yellow to brown-red starting at approx. 200 °C was obtained. Nevertheless, a constant boiling point could be determined.

Applicant's summary and conclusion

Executive summary:

The boiling point was determined experimentally with 278.2 °C (551.4 K) at atmospheric pressure 101100 Pa. This value is the mean of two independent determinations. Using the correction by Sidney Young, a boiling point at standard pressure of 278.4 °C (551.6 K) was calculated.

The experiment was performed using the SIWOLOBOFF method.

A change in colour from brown-yellow to brown-red starting at approx. 200 °C was obtained. Nevertheless, a constant boiling point could be determined.