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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 17 December 2008 and 27 January 2009.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
UK GLP standards (Schedule 1, Good Laboratory Practice Regulations 1999 (SI 1999/3106 as amended by SI 2004/0994)). Date of inspection: 21/08/008. Date of signature: 04/03/2009
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
4,4'-bis(methoxymethyl)-1,1'-biphenyl
EC Number:
700-008-0
Cas Number:
3753-18-2
Molecular formula:
C16 H18 O2
IUPAC Name:
4,4'-bis(methoxymethyl)-1,1'-biphenyl
Constituent 2
Reference substance name:
4,4-bis(methoxymethyl)-biphenyl
IUPAC Name:
4,4-bis(methoxymethyl)-biphenyl

Results and discussion

Boiling point
Boiling pt.:
369 K
Atm. press.:
102.65 kPa
Decomposition:
no

Any other information on results incl. tables

Thermographic data for Determinations 1 and 2 are shown in the tables below.

 

Thermographic Data – Determination 1

Thermal Event

Interpretation

Temperature

ºC

K

Endotherm

Onset of boiling

365.06

638

Atmospheric pressure: 102.65 kPa

Thermographic Data – Determination 2

Thermal Event

Interpretation

Temperature

ºC

K

Endotherm

Onset of boiling

365.44

639

Atmospheric pressure: 102.65 kPa

Mean boiling temperature: 639 ± 0.5 K

Applicant's summary and conclusion

Conclusions:
The boiling temperature of the test material has been determined to be 369 ± 0.5 K at 102.65 kPa.
Executive summary:

The determination was carried out by differential scanning calorimetry (DSC) using the procedure specified in ASTM E537-86, Method A2 Boiling Temperature of Council Regulation (EC) No 440/2008 of 30 May 2008. 

The boiling temperature of the test material has been determined to be 369 ± 0.5 K at 102.65 kPa.