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Melting point / freezing point

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Feb. 22 - Apr. 12, 2021; experimental phase: Mar. 1-5, 2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
Jul. 27, 1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Name: Zeocros CG180 (P Zeolite)
Batch no.: 2020-531
CAS no.: 1318-02-1
Composition: Zeolite (crystalline Aluminium silicate) 95-100 %
Storage: room temperature (20 ± 5 °C)
Expiry date: 1. Jan. 2022
Stability: stable under storage conditions
Appearance: off-white powder
Purity: not applicable, UVCB
Homogeneity: homogeneous
Production date: Dec. 2020
Molecular formula: not stated
Molecular weight: not stated
Vapour pressure: 0 hPa
Key result
Melting / freezing pt.:
> 600 °C
Atm. press.:
ca. 1 013 hPa
Decomposition:
no

Two DSC measurements were performed.

No endothermic event was detected in both measurements, except an unsteady baseline between 159.12 °C and 229.56 °C in the second measurement. The unsteady baseline could be a sign of splitting of a chemical compound.

Likewise, no signs of melting were seen when heated on magnesia groove.

Therefore, the melting point should be stated as >600 °C under these test circumstances.

Conclusions:
No clear event was detected during the DSC measurement, also no signs of melting were observed by heating the test item on a magnesia groove.
Therefore, the melting point of the test item Zeocros CG180 should be stated as > 600 °C.
Executive summary:

The determination of the melting point of Zeocros CG180 was determined via DSC (differential scanning calorimetry).

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Feb. 22 - Apr. 12, 2021; experimental phase: Mar. 1-5, 2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
Jul. 27, 1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Name: Sylosiv A4 (A Zeolite)
Batch no.: 1000361205
CAS no.: 1318-02-1
Composition: Zeolite (crystalline Aluminium silicate) 95-100 %
Storage: room temperature (20 ± 5 °C)
Expiry date: 31. Jan. 2022
Stability: stable under storage conditions
Appearance: off-white powder
Purity: not applicable, UVCB
Homogeneity: homogeneous
Production date: 1. Dec. 2020
EC no.: 215-283-8 (930-915-9)
Molecular formula: not stated
Molecular weight: not stated
Vapour pressure: 0 hPa
Key result
Melting / freezing pt.:
> 600 °C
Atm. press.:
ca. 1 013 hPa
Decomposition:
no

Two DSC measurements were performed.

No endothermic event was detected in both measurements, except an unsteady baseline between 152.82 °C and 232.21 °C in the second measurement. The unsteady baseline could be a sign of splitting of a chemical compound.

Likewise, no signs of melting were seen when heated on magnesia groove.

Therefore, the melting point should be stated as >600 °C under these test circumstances.

Conclusions:
No clear event was detected during the DSC measurement, also no signs of melting were observed by heating the test item on a magnesia groove.
Therefore, the melting point of the test item Sylosiv A4 should be stated as > 600 °C.
Executive summary:

The determination of the melting point of Sylosiv A4 was determined via DSC (differential scanning calorimetry).

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Feb. 22 - Apr. 12, 2021; experimental phase: Mar. 1-5, 2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
Jul. 27, 1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Name: Na Y Zeolite (Y Zeolite)
Batch no.: RZ200094/1
CAS no.: 1318-02-1
Composition: Zeolite (crystalline Aluminium silicate) 95-100 %
Storage: room temperature (20 ± 5 °C)
Expiry date: 31. Jan. 2022
Stability: stable under storage conditions
Appearance: off-white powder
Purity: not applicable, UVCB
Homogeneity: homogeneous
Production date: 01. Dec. 2020
EC no.: 215-283-8 (930-915-9)
Molecular formula: not stated
Molecular weight: not stated
Vapour pressure: 0 hPa
Key result
Melting / freezing pt.:
> 600 °C
Atm. press.:
ca. 1 013 hPa
Decomposition:
no

Two DSC measurements were performed.

In both measurements no endothermic event was detected, except an unsteady baseline between 141.52 °C (lowest value) and 212.83 °C (highest value). The unsteady baseline could be a sign of splitting of a chemical compound.

Likewise, no signs of melting were seen when heated on magnesia groove.

Therefore, the melting point should be stated as >600 °C under these test circumstances.

Conclusions:
No clear event was detected during the DSC measurement, also no signs of melting were observed by heating the test item on a magnesia groove.
Therefore, the melting point of the test item Na Y Zeolite should be stated as > 600 °C.
Executive summary:

The determination of the melting point of Na Y Zeolite was determined via DSC (differential scanning calorimetry).

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Feb. 22 - Apr. 12, 2021; experimental phase: Mar. 1-5, 2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
Jul. 27, 1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Name: KÖSTROLITH NaMSXP-TR (X Zeolite)
Batch no.: 2006090001
CAS no.: 1318-02-1
Composition: Zeolite (crystalline Aluminium silicate) 95-100 %
Storage: room temperature (20 ± 5 °C)
Expiry date: 31. Jan. 2022
Stability: stable under storage conditions
Appearance: off-white powder
Purity: not applicable, UVCB
Homogeneity: homogeneous
Production date: 24. Nov. 2020
EC no.: 215-283-8 (930-915-9)
Molecular formula: not stated
Molecular weight: not stated
Vapour pressure: 0 hPa
Key result
Melting / freezing pt.:
> 600 °C
Atm. press.:
ca. 1 013 hPa
Decomposition:
no

Two DSC measurements were performed.

In both measurements no endothermic event was detected, except an unsteady baseline between 142.03 °C (lowest value) and 248.75 °C (highest value). The unsteady baseline could be a sign of splitting of a chemical compound.

Likewise, no signs of melting were seen when heated on magnesia groove.

Therefore, the melting point should be stated as >600 °C under these test circumstances.

Conclusions:
No clear event was detected during the DSC measurement, also no signs of melting were observed by heating the test item on a magnesia groove.
Therefore, the melting point of the test item Köstrolith NaMSXP-TR should be stated as > 600 °C.
Executive summary:

The determination of the melting point of Köstrolith NaMSXP-TR was determined via DSC (differential scanning calorimetry).

Description of key information

The melting point of all tested zeolites was greater than 600 °C.

Key value for chemical safety assessment

Additional information

The melting point of all tested zeolites was greater than 600 °C.