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The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Between 08 October 2012 and 03 December 2012.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
yes
Type of method:
pour point

Test material

Constituent 1
Chemical structure
Reference substance name:
Phosphorodithioic acid, mixed O,O-bis(2-ethylhexyl and iso-Bu and pentyl) esters, zinc salts
EC Number:
273-527-9
EC Name:
Phosphorodithioic acid, mixed O,O-bis(2-ethylhexyl and iso-Bu and pentyl) esters, zinc salts
Cas Number:
68988-45-4
Molecular formula:
Not applicable
IUPAC Name:
Phosphorodithioic acid, mixed O,O-bis(2-ethylhexyl and iso-Bu and pentyl) esters, zinc salts
Details on test material:
Identification: A-197
Description: Pale brown liquid
Batch: B12-12212
Purity: 77 % in mineral oil
Expiry / Retest Date: 20 September 2013
Storage Conditions: Approximately 4 °C in the dark

Results and discussion

Melting / freezing point
Melting / freezing pt.:
258 K
Decomposition:
no
Sublimation:
no
Remarks on result:
other: The pour point of the test item has been determined to be -15 ± 3 °C (258 ± 3 K).

Any other information on results incl. tables

Results

The results are shown in Table 3.1.

 

Table 3.1

 

 

 Determination 1

Determination 2

Stationary point (°C)

-18

-18

Pour point (°C)

-15

-15

Applicant's summary and conclusion

Conclusions:
The pour point of the test item has been determined to be -15 ± 3 °C (258 ± 3 K).
Executive summary:
The determination was carried out using the pour point method, designed to be compatible with Method A1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Conclusion

The pour point of the test item has been determined to be -15 ± 3 °C (258 ± 3 K).