Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 236-615-8 | CAS number: 13450-99-2
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- January 22, 2014 - February 7, 2014
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: The study was performed in accordance with the EC A.1 and OECD 102 guidelines and complied with the principles of GLP.
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Version / remarks:
- (2008)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Version / remarks:
- (1995)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EPA OPPTS 830.7200 (Melting Point / Melting Range)
- Version / remarks:
- (1998)
- Deviations:
- no
- GLP compliance:
- yes
- Type of method:
- thermal analysis
- Remarks:
- (differential scanning calorimetry)
- Decomposition:
- yes
- Remarks:
- (slight)
- Decomp. temp.:
- >= 350 °C
- Remarks on result:
- other: The substance has no melting point
- Conclusions:
- No melting up to 400°C was observed for the substance using differential scanning calorimetry (GLP-compliant study in accordance with EC A.1, OECD 102 and EPA OPPTS 830.7200). Decomposition of the substance started at 350°C. The substance has no melting temperature.
Reference
PRELIMINARY TEST WITH TGA
No significant weight loss was observed up to approximately 350°C. At 550°C, the sample weight had decreased by 6.8%. After the experiment, a light grey residue remained in the sample container.
DSC EXPERIMENTS
No effects were observed up to 400°C which were due to melting of the test substance. After the experiment, an off-white residue remained in the sample container. The change of the colour indicated slightly reaction and/or decomposition of the test substance.
TGA/DSC curves: see attached document.
Description of key information
The substance has no melting temperature. Decomposition of the substance started at 350°C.
Key value for chemical safety assessment
Additional information
The melting point of the substance was determined using differential scanning calorimetry (GLP-compliant study in accordance with EC A.1, OECD 102 and EPA OPPTS 830.7200).
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
